John, Julien,
For the purpose of combining both EDS and WDS in PI, I understand that a sync pulse is required to be sent from the EPMA to the EDS hardware to synchronize the EDS data collection with stage/beam movement. I don't understand why one would still need a multiplexer? This would imply that one wants to send the WDS info to the EDS system. Do we need to do this when using PI? I guess this adds extra functionality for someone without PI, but I imagine if using PI, this is not required?
Assuming one wanted to send the WDS signals to the EDS hardware, would the multiplexer be needed on an EDS system with 5 wds inputs?
Gareth
It's a good question.
There are several ways to combine WDS and EDS acquisitions. Let's look at each of them.
1. Integrated WDS and EDS full spectrum point analyses.
With this method, implemented in Probe for EPMA, we can acquire a normal WDS point acquisition and also a full EDS spectrum (and soon a full CL spectrum!) for each data point. PFE can acquire full EDS spectra from Penepma12 (Demo mode), or Thermo NSS or Bruker Esprit using only a software API.
The WDS and EDS data is acquired on all samples (standards, unknowns and wavescans) and can be quantified for standards and unknowns using full k-ratios where the net intensities for the EDS elements are obtained from the Bruker or Thermo interface (no demo mode net intensity function as yet) in on-line or off-line mode (note Thermo NSS is free for data re-processing, Bruker Esprit is not). Full matrix and interference corrections are applied.
See here for more details:
http://probesoftware.com/smf/index.php?topic=79.02. Integrated EDS and WDS with Bruker or Thermo applications.
With this method, the WDS raw PHA counts are sent via a BNC cable (multiplexer hardware) to the Thermo or Bruker hardware and displayed in the Thermo NSS or Bruker Esprit application for x-ray maps only.
The WDS map data cannot be background corrected or quantified, only displayed in NSS or Esprit.
See here for more details:
http://probesoftware.com/smf/index.php?topic=134.0http://probesoftware.com/smf/index.php?topic=77.msg284#msg2843. Integrated WDS and EDS mapping in Probe Image (using ROI mapping inputs)
With this method, we utilize Probe Image to acquire WDS maps and if the Bruker (not available for Thermo) mapping outputs are available we can send those to the Cameca or JEOL mapping inputs and display the EDS ROI data along with the WDS maps in Probe Image.
As is the case with method #2, we cannot quantify the EDS maps.
At the current time, this only works for JEOL instruments and the JEOL EDS, though we will be implementing the EDS element ROIs mapping outputs at some point for Bruker EDS systems, but since the EDS maps cannot be quantified using this method, it is not a top priority.
See here for more details:
http://probesoftware.com/smf/index.php?topic=77.04. Integrated WDS mapping and EDS spectrum imaging in Probe Image.
The is the so called "holy grail" of EPMA where we acquire full WDS maps and at the same time, using a pixel sync pulse from the EPMA map scan generator, trigger a full EDS spectrum acquisition for every pixel, all fully synchronized. This is the subject of this topic.
Thermo and Bruker (and also JEOL) are currently working on implementing this "passive" WDS EDS mapping acquisition method using their hardware sync input and an API which I designed for obtaining the net intensity maps for quantitative post processing of the maps.
Using this method both the WDS and EDS map data can be fully quantified for background, matrix and interference effects using standard intensities from Probe for EPMA, maps from Probe Image and quantified using CalcImage.
I will be posting progress updates here.