I have a data acquisition request for our JEOL ProbeImage/CalcImage colleagues... but first some background.
As many of you already know, Probe for EPMA contains a very robust drift correction not only for beam current drift, but also for standard intensity drift. This beam current drift correction is commonly performed by other softwares, but the automatic standard intensity drift correction is unique to PFE, and allows the software to correct for changes in the measured standard intensities over time, on an element by element basis. That is, assuming that you acquired your standard(s) both before *and* after your unknown point acquisitions!
Now I have fully implemented this beam current and standard intensity drift correction in CalcImage for our x-ray mapping quantification. The beam current drift correction was already implemented in CalcImage but now, the standard intensity drift correction is also implemented. This standard intensity drift correction is a totally unique feature in both PFE and now, CalcImage, and it works amazingly well.
And because the standard intensity drift correction is performed on an element by element basis, it can deal with temperature related drift issues such as the thermal sensitivity of the PET crystals.
I also implemented the new CalcImage drift correction code so it automatically handles the situation where there is more than one x-ray map acquisition set for the quantification. That is, more than one element per spectrometer were acquired in Probe Image, using multiple sample acquisitions on the same area.
Cool.
So now I would like to obtain a small test dataset (MDB and PrbImg files) from a JEOL instrument (you'll see why in a second), on a homogeneous standard sample, for both a beam scan and a stage scan. Just 3 to 5 elements, and no need to acquire off-peak maps as I would like to test the MAN drift correction as well, so please also acquire the primary standards and the MAN stds in PFE, both *before* the x-ray maps are run, and again *after* the x-ray maps are acquired.
Ideally this would be an overnight mapping run where you observe significant drift in either or both the beam current and/or the standard intensities. A lab with significant temperature variation would be ideal.
Hopefully the beam current and standard intensity drifts are linear because all we can do is interpolate linearly between standardizations...
Now, why do I want only JEOL MDB and map data? Well because I'm calculating the drift by assuming the first pixel acquired is in the upper left of the map and the last pixel acquired is in the lower right. This exactly the case for all Cameca beam and stage scans, but is only the case for the JEOL beams scans. As you may know, JEOL stage scans start in the upper right and end in the lower left. It's an interesting story:
http://probesoftware.com/smf/index.php?topic=101.0I will need to add a case to handle beam current and standard intensity drift for JEOL stage scans, but right now I'd like to test the beam scan drift and use the stage scan for testing the next coding effort, that is once I figure a method for determining if the x-ray map was a JEOL beam or stage scan!
So here's the test acquisition protocol if you are interested:
1. Create a sample setup in Probe for EPMA with 3 to 5 elements (or more if you want to do a two pass acquisition with more than one element per spectrometer). Karsten has excellent documentation for this here:
http://probesoftware.com/smf/index.php?topic=106.02. Acquire your primary and MAN standards in PFE. They are automatically saved to your MDB file.
3. Acquire both a beam scan and a scan scan using this setup in Probe Image. Please name the beam scan sample "Beam scan..." and the stage scan "Stage scan...". The x-ray map PrbImg files are automatically saved.
4. Now acquire the primary and MAN standards in Probe for EPMA *again*, for the drift correction.
Hopefully even if the beam current and/or standard intensity drift was significant, we can now correct for this in CalcImage.
Feel free to play the the latest version of CalcImage yourself and test the new drift correction code, but please do send me a ZIP with the MDB and the PrbImag files acquired so I can try it myself.
Thank-you!
john